Ethyl Acetate Synthesis
Method of Synthesis of Ethyl Acetate
If you want to synthesize ethyl acetate, when the method is clear, it will be described below.

Acetic acid and ethanol can be combined in phases, using sulfuric acid as a catalyst. Mix the two, put them in an adapter, and add sulfuric acid to promote their response. Sulfuric acid can increase the speed of the reaction, but be careful when using it, because it is highly corrosive.

When reacting, its temperature needs to be controlled. Under moderate temperature, acetic acid and ethanol form ethyl acetate and water. The corresponding formula is as follows: $CH_ {3} COOH + C_ {2} H_ {5} OH\ underset {\ triangle} {\ overset {H_ {2} SO_ {4}} {\ rightleftharpoons}} CH_ {3} COOC_ {2} H_ {5} + H_ {2} O $.

After the reaction is completed, the product is mixed with acetic acid, ethanol and sulfuric acid. To obtain pure ethyl acetate, it is necessary to separate it. You can first wash it with a saturated sodium carbonate solution, which can remove acetic acid, dissolve ethanol, and reduce the solubility of ethyl acetate.

After washing, stratify it, and take ethyl acetate in the upper layer. However, the obtained product still contains trace amounts of water, which can be removed by desiccants such as anhydrous calcium chloride to obtain pure ethyl acetate.

This is a rough method for the synthesis of ethyl acetate. In practice, all details should be paid attention to in order to achieve its success.